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Ethylenediamine Processed Cu2SnS3 Nano Particles via Mild Solution Route

Ethylenediamine Processed Cu₂SnS₃ Nano Particles via Mild Solution Route

Department of Physics, Manonmaniam Sundaranar University, Tirunelveli- 627 012, Tamil Nadu, India

Centre for Scientific and Applied Research,School of Basic Engineering and Sciences, PSN College of Engineering and Technology, Tirunelveli – 627 152,Tamil Nadu, India

Department of Electrical and Computer Engineering, Ajou University, Suwon - 443 749, Republic of Korea

Centre for Instrumentation and Service Laboratory, Department of Physics, Annamalai University, Annamalai Nagar- 608 002, Tamil Nadu, India

Instituto de Energias Renovables- UNAM 62580,Temixco, Morelos,Mexico

Corresponding Author Email:

kmohanraj.msu@gmail.com, s_thanikai@rediffmail.com, sjp@ier.unam.mx

Received:

10 November 2015

| |

Accepted:

25 November 2015

| | Citation

v19n01a01_001-005.pdf

OPEN ACCESS

Abstract:

Copper tin sulphide nanoparticles have been prepared by solution growth technique at various ethylenediamine concentrations. Prepared samples have been characterized using x-ray diffraction, fourier transform infrared, Raman and scanning electron microscopy techniques. x-ray diffraction results revealed that the prepared samples are nanocrystalline in nature with tetragonal structure. Fourier transform infrared spectroscopy analysis results showed the presence of Cu-O, Sn-O and Sn-S vibrations in the wavenumber range between 450 and 620 cm^-¹. Vibrational symmetry of prepared samples have been analyzed using Raman spectroscopy. Scanning electron microscopy analysis indicated the formation of flower like nanocrystals for samples prepared at various Ethylenediamine concentrations.

Keywords:

Cu2SnS3, nanoparticles, solvothermal method, ethylenediamine

1. Introduction

2. Experimental Details

3. Results and Discussion

4. Conclusions

5. Acknowledgment

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Ethylenediamine Processed Cu2SnS3 Nano Particles via Mild Solution Route